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Pmove Operation Large Color-Display Transparent Draft Deflector Attachable Keyboard Barcode-Scanner USB Interface Manufacturer since 1873 WWW.PETROTEST.COM

Softening-Point Scope of Application To determine the temperature at which a substance attains a particular degree of softness. Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores. Summary of Method Two horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to 80 C in distilled water or silicone oil, above +80 C in glycerin or silicone oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm. Softening-Point - Ring & Ball Method - RKA 5 (automatic) Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53 EN 1427 (DIN 52 011, NF T66-008) IP 58 JIS K2207 Filler aggregats in bituminous mixtures: EN 13179-1 Wilhelmi-Option: DIN 1996-15 EN 1871-F Resins: ASTM E 28 Paints & Varnishes: ISO 4625-1 BS 6782-6 Thermoplastic Adhesives: EN 1238 (NF T76-106) Petrotest Ball Dispense & Centering Device (10-0840) (convenient Petrotest setup, included in standard delivery) PMove Jog-Wheel operation system Standard Ball Centering Device (10-0841 & 2x 10-0052) (a standard setup with centering guides, substitutional for 10-0840) 2 The RKA 5 instrument features a microprocessor technology combined with a smart jog-wheel operation system. It maintains program sequences for all relevant test standards and bath liquids as well as for user defi ned test conditions. An infrared radiator along with a controlled magnetic stirrer ensure the optimum test conditions, the four-wire Pt-100 and the laser-based ball detection probe guarantee precise test results. A draft deflector stabilizes ambient and homogeneous heating conditions, the lifting traverse simplifi es setup and handling of the test rack. An optional automatical system leads and dispenses the balls to the specimens. The test procedure is supported by intelligent software routines, at the end an automated test assessment is done. Heat gradients are precisely recorded and are available as printouts. Test results can be stored in the instrument and / or transferred via USB. Keyboard or barcode scanner options are avaiable as input support.

Softening-Point Dispensed Balls Laser-Scanner Main Units 10-0800 10-0801 RKA 5 - Automatic Softening-Point Tester Ring and Ball Method ASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (With optional accessories for: EN-1871-F (DIN 1996-15) or referee tests acc. IP & NF) Further for resins (ASTM E 28), paints and varnishes (ISO 4625-1 - BS 6782-6) and thermoplastic adhesives (EN 1238 (NF T76-106)) Features: Pmove - innovative operation platform large color display - visible from 10 m (30 ft.) easy Firmware-upload via USB compact ball detection system Ready-to-Go unit for two simultaneous tests CPU: Up-to-date dual OMAP controller technology featuring a real-time DSP and a multimedia coprocessor, 4.7 full graphical color display, graphical menu guidance and intuitive user concept (Pmove ), help key (explanation of important device/ program features), Jog-Wheel operation (turn & push), large-area device status indicator (light ring), zooming temperature reading, device & data management via LAN, USB or RS232, extended statistical and database functionality, automatic assessment of results according to individual standards, printout on heat gradient conformity. Electronic device features: Automatic self check of sensors and system, multipoint calibration of temperature sensor (Pt-100), compact ball sensing system consisting of a precise 3D-adjustable laser scanner. Mechanical device features: Infrared radiator technology with temperature control, CERAN heat plate, standardized beaker with barcode imprint, test rack with slide bearing and single-hand fi xation, Pt-100 gold plated fourwire system (also available with calibration certifi cate), test rings, load balls, centering guides, stirring wheel, holding tong, mechanical ball centering system, software controlled stirrer system, transparent draft defl ector. Supplied with: 10 rings (shouldered), 10 load balls, 1 gauge ball, 1 test rack with mechanical ball centering unit (standard type upon request), 1 glass-beaker bath (600ml) with barcode, 1 tongs (aluminum), 1 temperature probe (Pt-100) and 1 test tube (as Pt-100 tray), 1 magnetic stirrer (ring shape), 1 pouring plate (brass) Note: Accessories like electromagnetic ball & centering unit, external USB-keyboard, barcode scanner, printer (USB, serial), memory stick, bath liquid and optional test accessories are not included. Technical Data: Test places : 2 (for simultaneous tests) Housing : stainless steel, two colored powder coating Interface : 1 serial RS232, 3 USB, 1 LAN (LIMS) Dimensions : 230 x 470 x 460 cm (WxDxH), Weight: 10 kg Power supply : 230 V, 50/60 Hz, EU-plug Power supply : 115 V, 50/60 Hz, US-plug Selection of Program Selection of Standard Display of Results 3

Options Electromagnetic Ball Dispense (comfortable Petrotest setup) Manual Standard Ball Dispense (standard setup with centering guides) RKA & 10-0851 & 25-0910 & 25-0920 Accessories 25-0910 Keyboard, USB, 86 keys, illuminated 25-0920 Barcode-Scanner, USB 25-0919 Memory Stick, 2 GB, USB 2.0 (verifi ed for Petrotest -units) Mechanical Petrotest Ball Dispense (very convenient Petrotest setup) 25-0930 25-0282 25-0283 Impact Printer for single sheet & continuous paper, serial Power supply : 220/240 V, 50/60 Hz Power supply : 110/130 V, 50/60 Hz 25-0900 Laser Printer (Mono) for single sheet, USB Power supply : 220/240 V, 50/60 Hz 25-0930 Receipt Impact Printer (POS) for paper rolls, serial Power supply : 120/230 V, (AC converter output 7 V) 50-9160 51-9151 Bath Liquid, silicone oil M50, 1 kg, water clear, heat resistant up to approx. +200 C glycerin, 99% pure, 1 kg 10-0070 Mortar with pestle (acc. ISO 4625, ASTM E 28) 10-0868 Service Kit RKA 5 Consisting of 1 each: reference plug 20 C & 180 C, scanner & ball gauge, visor, USB-memory stick, SD card, scraper, plastic cleaner and tool set (8 mm combination wrench, crosstip & 8 mm hex ball screwdrivers) Service Kit 10-0868 10-0049 Rings, shouldered, nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF) 10-0805 Load Balls, blackened steel (Ø 9.5 mm, 3.5 g), pack of 10 10-0856 Glass Beaker (600 ml) with barcode (as bath) 50-5227 Magnetic Stirrer Ring (Ø 57 mm) 50-5317 Tongs for beaker (aluminum) 4 50-5317 10-0079 Pouring Plate, brass, U-shape (50 x 75 mm) to fi ll the rings 10-0840 Test Rack RKA 5-Dispensing Device with mechanical Petrotest ball centering & dispensing device 10-0849 Temperature Probe Pt-100 17-0158 Test Tube, borosilicate glass (to hold the ball dispenser or Pt-100) 10-0888 Gauge-Ball RKA 5 for light barrier adjustment

10-0860 10-0864 Test Rack with: mechanical Petrotest ball centering & dispense device (10-0840 and accessories) Test Rack for use with: - standard ball centering guides (10-0841, 2x 10-0052) - in combination with electromagnetic ball dispensers & guides (10-0851) Modifi ed Test Rack with accessories similar to Wilhelmi Method (10-0860 & 10-0864) 10-0888 Mechanical Ball Centering & Dispense Device (included in the standard delivery) 10-0840 Test Rack RKA 5-Dispensing Device with mechanical Petrotest ball centering & dispensing device Accessories 10-0805 Load Balls, blackened steel (Ø 9.5 mm, 3.5 g), pack of 10 Manual Ball Dispense Option (to be ordered as replacement for the incl. 10-0840) 10-0841 Test Rack RKA 5-Centering Guide to be used with 2 ball centering guides 10-0052 Ball Centering Guide for shouldered rings Electromagnetic Ball Dispense Option 10-0851 Test Rack Kit RKA 5 Electromagnetic for electromagnetic ball dispensing 1 test rack for centering guides 2 electromagnetic ball dispensers 2 test tubes, as ball dispenser holder 2 ball centering guides Accessories 10-0049 Rings, shouldered, nickel-plated brass, pack of 10 10-0805 Load Balls, blackened steel (Ø 9.5 mm, 3.5 g), pack of 10 10-0052 Ball Centering Guide 10-0841 Test Rack RKA 5-Centering Guide to be used with 2 ball centering guides & 2 ball dispensers 10-0850 Ball Dispenser, electromagnetic 17-0158 Test Tube, borosilicate glass (to hold the ball dispenser or Pt-100) 10-0856 (& stirrer ring) 10-0052 & 10-0049 Wilhelmi-Method Option (for manual or automatic ball detection) 10-0860 Test Rack Kit RKA 5 Wilhelmi - manual detection (EN 1871 / DIN 1996-15) used for Mastix determination 10-0075 10-0877 Ring (Wilhelmi) with bayonet lock Load Balls (Wilhelmi), blackened steel (Ø 15 mm, 13.9 g), pack of 10 1 test rack 10-0906 Glass Beaker (Wilhelmi) (1000 ml) 1 ring with bayonet lock with barcode (as bath) 10 load balls (Ø 15 mm, 13.9 g) 1 magnetic ball dispenser 10-0846 Temperature Probe (Wilhelmi) Pt-100 1 temperature probe Pt-100, (fi ts 10-0860 only) 1 glass beaker (1000 ml) 10-0865 Ball Dispenser (Wilhelmi), magnetic 1 pouring plate (50 x 75 mm) 1 Allen key (2 mm) 17-0237 Allen Key (2 mm) 10-0079 & Rings 10-0864 Test Rack Extension RKA 5 Wilhelmi - automatic detection (similar to EN 1871 / DIN 1996-15) requires Test Kit 10-0860 1 rod (50 mm) 1 bottom plate, perforated 2 distance pieces (25 mm) 10-0861 Test Rack RKA 5-Wilhelmi for manual ball detection Load Balls (for RKA5 instruments only) (10-0805 & 10-0877) Option former referee tests acc. IP 58 & NF T66-008 10-0048 Rings, tapered (former IP & NF), pack of 10 10-0051 Ball Centering Guide for tapered rings (former IP & NF) 10-0051 & 10-0048 5

Scope of Application To determine the temperature at which a substance attains a particular degree of softness. Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores. Summary of Method Two horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to +80 C in distilled water or silicone oil, above +80 C in glycerin or silicone oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm. Softening-Point - Ring & Ball Method (manual) Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53 EN 1427 (DIN 52 011, NF T66-008) - IP 58 JIS K2207 Filler aggregats in bituminous mixtures: EN 13179-1 (Wilhelmi-Option: see next page) Main Units Manual Softening-Point Tester, Ring & Ball Method ASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (with optional accessories for referee tests acc. IP & NF) Further for resins (ASTM E 28), paints and vanishes (ISO 4625-1 - BS 6782-6) Features: 2 simultaneous tests electric heating electric stirrer electric heater (800 W) in stainless steel housing with electronic power regulator, 4 heater rods, electric stirrer and support for two test rings Supplied with: 10 shouldered rings, 10 load balls, 2 ball centering guides, 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (600 ml), 1 heater support board (bored, 50 mm / 2 ), 1 pouring plate (brass), 1 mortar with pestle Technical Data: Test places : 2 Working range : approx. +25 to +200 C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kg 10-0281 Power supply : 230 V, 50/60 Hz, 800 W, EU-plug 10-0284 Power supply : 115 V, 50/60 Hz, 800 W, US-plug Options & Accessories 50-5315 Tongs for beaker 50-9167 Bath Liquid, silicone oil, water clear, 1 kg, water clear, heat resistant up to approx. +250 C, viscosity at +25 C: 190 till 210 mpa s For former referee tests acc. IP 58 & NF T66-008: 10-0048 Rings, tapered (former IP & NF), pack of 10 10-0051 Ball Centering Guide for tapered rings (former IP & NF) 10-0281 Thermometers Precision Made Officially Certified Type ASTM IP Range 10-0061 10-0062 15C 60C -2 to +80 : 0.2 C 10-0063 10-0064 15F - +30 to +180 : 0.5 F 10-0065 10-0066 16C 61C +30 to +200 : 0.5 C 10-0067 10-0068 16F - +85 to +392 : 1.0 F 6 Ring & Ball Accessories 50-5315 10-0052 Ball Centering Guide for shouldered rings 10-0055 Load Balls, steel (Ø 9.5 mm, 3.5 g), pack of 10 10-0049 Rings, shouldered, nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF) 10-0455 Ring-Holder Assembly for 2 rings 10-0056 Glass Beaker (600 ml) as bath 10-0070 Mortar with pestle (ISO 4625, ASTM E 28) 10-0079 Plate, brass, U-shape (50 x 75 mm) as pouring plate to fi ll the rings 11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm), with center hole (Ø 50 mm / 2 ) 11-0018 Heater Rod, 200 W, 115-230 V 11-0019 11-0029 25-0004 25-0009 25-0042 25-0043 Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W... 115 V, 50/60 Hz, 800 W Control Module M2 to regulate the heating power... 230 V, 50/60 Hz... 115 V, 50/60 Hz Electric Stirrer with propeller blade... 230 V, 50/60 Hz, EU-plug... 115 V, 50/60 Hz, US-plug

Softening-Point - Wilhelmi Method (manual) Bituminous materials: DIN 1996-15 Thermoplastic materials: EN 1871-F Main Unit 10-0071 Manual Softening-Point Tester, Wilhelmi Method Features: single test place electric heating electronic power regulator electric heater (800 W) in stainless steel housing with electronic power regulator M2, 4 heater rods, laboratory stand (1 bar, 1 special clamp, 1 ring support) Supplied with: 1 Wilhelmi ring, 10 load balls 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (1000 ml), 1 heater support board (bored, 50 mm / 2 ), 1 pouring plate (glass) Technical Data: Test place : 1 Working range : approx. +25 to +200 C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kg Power supply : 230 V, 50/60 Hz, 800 W, EU-plug Scope of Application To determine the temperature at which a hot casting substance used in road construction attains a particular degree of softness. Suitable for joint sealing compounds in road construction and thermoplastic materials for pavement marking. Summary of Method A horizontal disk of a sample casted in a ring supports a steel ball and is heated at a controlled rate in a liquid bath (up to +80 C in distilled water or silicone oil, above +80 C in glycerin or silicone oil). The softening-point is reported as the temperature at which the softening disk experiences a plastic deformation. Options & Accessories 50-5315 Tongs for beaker 50-9167 Bath Liquid, silicone oil, water clear, 1 kg, heat resistant up to approx. +250 C, viscosity at +25 C: 190 till 210 mpa s For automatic tests see Ring & Ball-Apparatus RKA 5: 10-0800 RKA 5 - Automatic Softening-Point Tester, Ring & Ball Method 10-0860 Test Rack Kit RKA 5 acc. Wilhelmi Thermometers Precision Made Officially Certified Type ASTM IP Range 10-0061 10-0062 15C 60C -2 to +80 : 0.2 C 10-0063 10-0064 15F - +30 to +180 : 0.5 F 10-0065 10-0066 16C 61C +30 to +200 : 0.5 C 10-0067 10-0068 16F - +85 to +392 : 1.0 F 10-0071 10-0077 Load Balls (Wilhelmi), steel (Ø 15 mm, 13.9 g), pack of 10 10-0075 Rings (Wilhelmi) with bayonet lock 10-0076 Ring-Holder (Wilhelmi) 10-0106 Glass Beaker with spout (1000 ml) low shape, as bath 10-0057 Plate, glass (120 x 120 x 6 mm) as pouring plate to fi ll the rings 11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm) with center hole (Ø 50 mm / 2 ) 11-0018 Heater Rod, 200 W, 115-230 V 11-0019 25-0004 Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W Control Module M2 to regulate to heating power... 230 V, 50/60 Hz Wilhelmi Ring (10-0075) Load Balls (for manual instruments only) (10-0055 & 10-0077) 7

Manufacturer of Petroleum Test Equipment since 1873 Petrotest Building Development ISO 9001 certified processes......all under one roof! Production Quality Control Storage training Presented by: We reserve the right of changes without prior notice. 98-1430 10/04 Ludwig-Erhard-Ring 13 15827 Dahlewitz - Germany Tel.: +49 (0) 33708 / 56-300 Fax: +49 (0) 33708 / 56-556 e-mail: info@petrotest.com website: www.petrotest.com