Genevac Accessories and Spares For Rocket Synergy Evaporators Original instructions in English 04-8931 Issue 1-14 October 2015
Contents Introduction... 2 Maintenance of sample holders... 2 Limitations of use... 3 Colour variation of surface finish... 3 Rotors... 4 Flask rotor... 4 Bowl rotor... 4 Rotor Spares... 5 Rotor accessories... 7 Sample Holders for Flask Rotors... 8 SampleGenie 4... 8 SampleGenie 4 spares... 9 GC Vial System 2... 12 GC Vial System 2 spares... 13 Standard Flask... 15 Standard flask spares... 15 ASE Tube Puck... 16 ASE Tube Puck spares... 16 Flip-Flop... 17 Flip-Flop Spares... 18 Accessories... 20 Sampleholder accessories... 20 Infinity Trolley... 21 General Spares... 22 Main lid seal... 22 Sample viewing window... 22 Waste solvent container... 22 Lid joint coupling (for feed system)... 22 Feed hoses... 23 Fittings for coolant, drain and exhaust hoses... 23 Quick Reference... 24 s... 24 Amendment control... 25
Introduction Genevac produce a range of sample holders and accessories that can be used to enhance the performance and increase the flexibility of Rocket Synergy and Rocket 4D Synergy high speed evaporation systems. Sample holders are manufactured using high quality materials such as boroscilicate glass and high grade alluminium. Where applicable, seals can be specified in low leachable viton or in highly resistant perfluoroelastomer. Maintenance of sample holders The Rocket evaporator controls pressure levels in inner and outer vacuum chambers independently and sample holders form part of the seal between these chambers; it is therefore vitaly important that a perfect seal is formed around each of the sample holders. To achieve this, the sample holders must be maintained in good condition and must be used correctly. Sample holders must be clean and free from imperfections around the area of the sealing surfaces; chips, scratches or labels applied to the flasks may cause leaks which can slow down the evaporation process. Refer to the Genevac Rocket Sample Holders User Manual for advice on day to day maintenance and use of the Rocket sample holders. 2 04-8931 Issue 1-14 October 2015
Limitations of use This brochure contains informantion on a range of accessories and sample holders that are intended for use with Rocket Synergy and Rocket 4D Syenrgy evaporators. Some of the accessories and sample holders are also compatible with earlier ( pre-synergy ) Rocket evaporators, although limitations may apply. Where limitations do apply, they shall be indicated as shown in the following example: For use with Rocket 4D Synergy feed systems only In this example, the accessory must not be used with any system other than that which is specified. Colour variation of surface finish For some components the colouring of surface finish may vary slightly from batch to batch; for instance, one batch of vial adapters may appear darker than another. Where this occurs it does not affect the performance or integrity of the component. 04-8931 Issue 1-14 October 2015 3
Rotors Flask rotor Flask rotor 70-1734/S Six position flask rotor assembly for Rocket Synergy or Rocket 4D Synergy includes inner lid and six blanking plugs. Bowl rotor - batch Bowl rotor - batch 70-1820/S Five litre bowl rotor for Rocket 4D Synergy or Rocket Synergy, includes batch (non-feed) inner lid, batch baffles, lifting handles and USB data-key with Rocket Synergy batch methods. Bowl rotor - feed Bowl rotor - feed 70-1752/S Five litre bowl rotor for Rocket 4D Rocket 4D Synergy, includes feed inner lid, feed baffle, lifting handles and USB data-key with Rocket Synergy feed methods. 4 04-8931 Issue 1-14 October 2015
Rotor Spares Inner lid Non-feed 70-1548/S Inner lid for flask or non-feed bowl rotor. Inner lid Feed 70-1547/S Inner lid for bowl rotor For use with Rocket 4D Synergy feed systems only. Batch baffle 70-1549/S Batch baffle for bowl rotor. Set of two. Feed baffle Single feed baffle for bowl rotor. 04-7652/S 04-8931 Issue 1-14 October 2015 5
Inner lid seal 04-7448/S Seal for inner lid, fits flask rotor and bowl rotor. Flask seals 70-1180 Flask seals used on Rocket Synergy flask rotor and pre-synergy Rocket. O-ring 04-5676 O-ring (viton) for rotor hub. Seal Seal 70-1556/S Seal kit (consisting of plug and O-ring) for bowl rotor pouring spout. Cap Cap Cap for bowl rotor pouring spout. 70-1557/S 6 04-8931 Issue 1-14 October 2015
Rotor accessories Lid stand 70-1186 Stand for inner lid. Suitable for use with all variants. Lifting handles 70-1552/S Lifting handles for Rocket Synergy bowl rotor. Set of two. Blanking plug 70-2004/S Blanking plug for flask rotor. Set of two. Pouring stand 70-1798 Pouring stand. Suitable for use with bowl rotors that have a pouring spout. Synergy methods 04-8844 USB data key (flash-drive) containing method files for Rocket Synergy flask rotor and Rocket Synergy bowl rotor feed and batch methods. 04-8931 Issue 1-14 October 2015 7
Sample Holders for Flask Rotors SampleGenie 4 SampleGenie 4 70-1740 SampleGenie 4 flask assembly. For use in Rocket Synergy evaporators and Rocket 4D Synergy evaporators with optional flask rotor. Evaporators with serial numbers lower than RK0399 (pre-synergy) require low speed upgrade. Note: Excludes vial adapter, vial adapter pad and vial seal. When ordering: please select vial adapter from table below. Information on vial seals can be found in the following section: Sample Holder Spares. Vial adapter Vial adapter for SampleGenie 4. Note: Includes vial adapter pad. Max vial diameter ( mm) Vial length (mm) Seal required DG 15.3 36.5 to 41.5 One part 70-1766 DD 15.3 41.5 to 46.5 One part 70-1763 DJ 17.3 46.5 to 51.5 Two part 70-1769 DC 17.3 56.5 to 61.5 One part 70-1762 DH 20.8 39.5 to 44.5 Two part 70-1767 DF 23.3 42.5 to 47.5 Two part 70-1765 DI 23.2 54.5 to 59.5 Two part 70-1768 DE 23.3 66.5 to 71.5 Two part 70-1764 DB 28.0 56.5 to 61.5 Two part 70-1761 DA 28.0 66.5 to 71.5 Two part 70-1760 8 04-8931 Issue 1-14 October 2015
SampleGenie 4 spares SG 4 Flask 70-1741 Flask assembly only, for SampleGenie 4. Collar pad 70-1743 Collar pad for SampleGenie 4. Collar 70-1742 Collar for SampleGenie 4. Holder 70-1744 Holder for SampleGenie 4 vial adapter. Set of six 04-8931 Issue 1-14 October 2015 9
Insert 70-1757 Insert for SampleGenie 4 two-part vial seal. For use with viton vial seal: 70-1758 or perfluoroelastomer vial seal: 70-1759. Vial seal 70-1758 Viton Viton seal for SampleGenie 4 two-part vial seal. Requires insert: 70-1757. Note: Green mark in periphery indicates perfluoro. Note: Notch in periphery indicates perflouro. Vial seal 70-1759 Perfluoroelastomer Perfluoroelastomer seal for SampleGenie 4 two-part vial seal. Requires insert: 70-1757. Vial seal 70-1196 White viton One-part, low leachable white viton, vial seal for use with SampleGenie 4 Vial seal 70-1197 Perfluoro One-part, highly resistant perfluoroelastomer, vial seal for use with SampleGenie 4 10 04-8931 Issue 1-14 October 2015
Diameter Vial adapter pad 70-1745 16 mm Vial adapter pad for SampleGenie 4. Diameter Vial adapter pad 70-1746 18 mm Vial adapter pad for SampleGenie 4. Diameter Vial adapter pad 70-1747 24 mm Vial adapter pad for SampleGenie 4. Diameter Vial adapter pad 70-1748 28 mm Vial adapter pad for SampleGenie 4. 04-8931 Issue 1-14 October 2015 11
GC Vial System 2 GC Vial System 2 70-1423 Viton seals GC Vial System 2 flask assembly with low leachable white viton vial seals. GC Vial System 2 70-1424 Perfluoro seals GC Vial System 2 flask assembly with highly resistant perfluoroelastomer vial seals. 12 04-8931 Issue 1-14 October 2015
GC Vial System 2 spares GC 2 Flask 70-1425 Flask only, for GC Vial System 2. Vial seal 70-1177 White viton Low leachable white viton vial seal for GC Vial system 2. Note: Notch in periphery indicates perfluoro. Vial seal 70-1178 Perfluoro Highly resistant perfluoroelastomer vial seal for GC Vial System 2. 04-8931 Issue 1-14 October 2015 13
Vial adapter 70-1800 Two-piece vial adapter with O-ring, for CG Vial System 2 (backward compatible with all CG Vial System 2 flask aseemblies, replaces one-piece vial adapter: 70-1428) O-ring 70-1801 O-ring for CG Vial System 2 vial adapter: 70-1800. Collar pad 70-1317 Collar pad for GC Vial System 2. GC 2 collar 70-1320 Collar for GC Vial System 2. Cap 70-1176 Cap for GC Vial System 2. 14 04-8931 Issue 1-14 October 2015
Standard Flask Standard flask assy 70-1321 Standard Flask with collar pad and collar. Standard flask spares Standard flask 70-1170 Standard evaporation flask only. Collar pad 70-1317 Collar pad for standard flask. For evaporators with serial numbers below RK0133, flask adapters must be removed from the rotor. Collar 70-1319 Collar for standard flask. For evaporators with serial numbers below RK0133, flask adapters must be removed from the rotor. 04-8931 Issue 1-14 October 2015 15
ASE Tube Puck Puck 70-1282 ASE* tube puck assembly. ASE Tube Puck spares Puck seal 70-1287 Seal (viton O-ring) for ASE tube puck. Set of 18. 16 04-8931 Issue 1-14 October 2015
Flip-Flop Flip-Flop 70-1295 Viton seals Flip-Flop assembly with low leachable white viton seals. For use with ASE tube puck. Set of 18. Flip-Flop 70-1296 Perfluoro seals Flip-Flop assembly with highly resistant perfluoroelastomer seals. For use with ASE tube puck. Set of 18. *ASE is a registered trademark of Dionex Corporation. 04-8931 Issue 1-14 October 2015 17
Flip-Flop Spares Flip-Flop tube 70-1297 Double ended tube for Flip-Flop. Pack of 100 (plus 10 spare). Tube seal 70-1304 White viton Low leachable white viton tube seal for Flip-Flop (tube to funnel). Pack of 20. Tube seal 70-1306 Perfluoro Highly resistant perfluoroelastomer tube seal for Flip-Flop (tube to funnel). Pack of 20. Funnel 70-1298 Funnel for Flip-Flop. Pack of 18. O-ring 70-1299 O-ring for Flip-Flop (funnel to vial cover). Pack of 20. 18 04-8931 Issue 1-14 October 2015
Vial seal 70-1303 White viton Low leachable white viton vial seal for Flip-Flop. Pack of 20. Note: Notch in periphery indicates perfluoro. Vial seal 70-1305 Perfluoro Highly resistant perfluoroelastomer vial seal for Flip-Flop. Pack of 20. Ejector peg 70-1301 Vial ejector peg for Flip-Flop. Set of 18. O-ring 70-1302 O-ring for Flip-Flop vial ejector peg. Pack of 20. Vial cover 70-1300 Vial cover for Flip-Flop. Set of 18. 04-8931 Issue 1-14 October 2015 19
Accessories Sampleholder accessories Flask carrier 70-1187 Coated steel flask carrier for safe transportation or storage of six standard flasks, CG vial system flasks or SampleGenie flasks. Flask stand 70-1797 Single flask stand for use as a balance nest with: standard flask, GC Vial system flask or SampleGenie flask. Splash cap 70-1265 Viton splash cap for use with: standard flask, GC vial system flask or SampleGenie flask. Seal tool 04-8321 Tool for safe removal of vial seal from SampleGenie flask or GC vial system flask, without risk of damage to flask or seals. 20 04-8931 Issue 1-14 October 2015
Infinity Trolley Trolley 70-1650 Infinity Trolley for Rocket and Rocket Synergy. Accommodates one Rocket high speed evaporator, Julao FL601 re-circulating chiller and five litre waste solvent container. Trolley 70-1630 Infinity Trolley for Rocket 4D and Rocket 4D Synergy. Accommodates one Rocket 4D and Julabo FL1701 recirculating chiller. Shelf 70-1635 Shelf kit for Infinity Trolley. Accommodates one Edwards nxds6i vacuum pump or may be used as sample preparation area. 04-8931 Issue 1-14 October 2015 21
General Spares Main lid seal Main lid seal 04-5818/S Seal for main (outer) lid for Rocket Synergy, Rocket 4D Synergy and pre- Synergy Rockets. Sample viewing window Window 70-1182 Sample viewing window and gasket assembly for systems with strobe. Waste solvent container Waste container 5 litre 70-1247/S Waste solvent container kit comprising polypropylene waste solvent container, two port cap, drain hose (five metres) and fittings. Lid joint coupling (for feed system) O-ring 04-7943 O-ring (green perfluoroelastomer) for lid joint coupling (of feed system). 22 04-8931 Issue 1-14 October 2015
Feed hoses Feed hose Replacement feed hose. 50 metre length. 70-1553/S Fittings for coolant, drain and exhaust hoses Hose fittings 70-1651/S Hose fittings kit comprising two type 1A fittings and two type 2N fittings for coolant, drain and exhaust hose connections. 04-8931 Issue 1-14 October 2015 23
Quick Reference s 04-1247/S... 22 04-5676... 6 04-5818/S... 22 04-7448/S... 6 04-7652/S... 5 04-7943... 22 04-8321... 20 04-8844... 7 04-8850/S... 7 70-1170... 15 70-1176... 14 70-1177... 13 70-1178... 13 70-1180... 6 70-1182... 22 70-1186... 7 70-1187... 20 70-1196... 10 70-1197... 10 70-1265... 20 70-1282... 16 70-1287... 16 70-1295... 17 70-1296... 17 70-1297... 18 70-1298... 18 70-1299... 18 70-1300... 19 70-1301... 19 70-1302... 19 70-1303... 19 70-1304... 18 70-1305... 19 70-1306... 18 70-1317... 14, 15 70-1319... 15 70-1320... 14 70-1321... 15 70-1423... 12 70-1424... 12 70-1425... 13 70-1547/S... 5 70-1548/S... 5 70-1549/S... 5 70-1552/S... 7 70-1553/S... 23 70-1556/S... 6 70-1557/S... 6 70-1630... 21 70-1635... 21 70-1650... 21 70-1651/S... 23 70-1734/S... 4 70-1740... 8 70-1741... 9 70-1742... 9 70-1743... 9 70-1744... 9 70-1745... 11 70-1746... 11 70-1747... 11 70-1748... 11 70-1752/S... 4 70-1757... 10 70-1758... 10 70-1759... 10 70-1760... 8 70-1761... 8 70-1762... 8 70-1763... 8 70-1764... 8 70-1765... 8 70-1766... 8 70-1767... 8 70-1768... 8 70-1769... 8 70-1797... 20 70-1798... 7 70-1800... 14 70-1801... 14 70-1820/S... 4 24 04-8931 Issue 1-14 October 2015
Amendment control Issue Reason for Change Date Issued 1-1 First release 19-Dec-14 1-2 70-1759 images updated. Serial number limit for pre-synergy 08-Jan-15 systems added. 1-3 SG4 vial seal part number correction and duplications removed. 09-Jan-15 Flip-Flop vial seal part number changed for pack of 20. Perflouro identification notes added. 1-4 70-1196, 70-1197, 70-1177, 70-1178 reintroduced. Also used in 29-Jan-15 comments removed. Rotor hub O-ring removed. 1-5 Waste connection kit part number corrected. 17-Feb-15 1-6 04-5676, 04-7943, 70-1557/S included. 26-Mar-15 1-7 Pouring stand for bowl rotor part number updated to reflect design 30-Apr-15 change. Flask stand (balance nest) part number updated. 1-8 SG4 vials adapter DJ introduced. 14-May-15 1-9 70-1820/S introduced. Batch baffles added to 70-1820/S, feed 22-May-15 baffles added to 70-1752/S. 1-10 GC Vial System 2 vial addapter: 70-1800 replaces 70-1428, 70-1801 30-Jul-15 replaces 70-1429. 1-11 Address: SpScientific replaces SP industries. 10-Aug-15 1-12 Cap separated from GC Collar 2 ; added as separate item. 27-Aug-15 1-13 V3 Blanking Plug added. 30-Sept-15 1-14 Minor correction. 07-Oct-15 04-8931 Issue 1-14 October 2015 25
Genevac Ltd The Sovereign Centre Farthing Road Ipswich IP1 5AP United Kingdom Service: +44 (0) 1473 243000 Sales: +44 (0) 1473 240000 Fax: +44 (0) 1473 461176 Email: salesinfo@genevac.co.uk service@genevac.co.uk applications@genevac.co.uk Web site: http://www.genevac.com Genevac Ltd operates a continuous development programme aimed at further improving products, all specifications are therefore subject to change. Coolheat VacRamp, Dri-Pure, SampleGuard, SampleGenie and associated logos are trade-marks of Genevac Ltd, unauthorised use is prohibited. Your Genevac Sales Representative will be happy to advise on the availability of special order items in addition to the sample holders listed in this Accessories Brochure All rights reserved, Genevac Ltd 2015. Genevac Inc SP Scientific 3538 Main Street Stone Ridge NY12484 United States of America Sales & Service: (1) 845 267 2211 Fax: Fax (1) 845 267 2212 Email: sales@genevacusa.com